M-006 & M-007 In-Line Sample Concentration or Filtration
From LEAP
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[[Image:Empty TRIO.png|left frame|TrioVS valve is used. Flow path intentionally left incomplete. Contact LEAP for more information]] | [[Image:Empty TRIO.png|left frame|TrioVS valve is used. Flow path intentionally left incomplete. Contact LEAP for more information]] | ||
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| + | === Useful links === | ||
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| + | www.appliedbiosystems.com '''Application Note''' [http://www3.appliedbiosystems.com/cms/groups/applied_markets_marketing/documents/generaldocuments/cms_043785.pdf] | ||
| + | <br><br><br> | ||
| + | [[Image:HTC_with_TRIO.png]] | ||
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Revision as of 19:33, 2 June 2009
| In-Line Sample Concentration or Filtration |
| Application Type | |
| SPECIAL | |
| Application ID | |
| M-006 & M-007 | |
| Description | |
| In-Line Sample Cleanup |
| Code | Application | Control SW | Key Hardware | Key Benefits | Restrictions | GLP |
|---|---|---|---|---|---|---|
| M-006 | Inline Sample Concentration SPE Column regenerated during analytical extraction | Analyst with ICC-CE | * TrioVS | * Automated concentration and elution of sample on SPE column prior to separation on analytical column | * No "Look Ahead" * Can not prep samples ahead of analytical run | No |
| Code | Application | Control SW | Key Hardware | Key Benefits | Restrictions | GLP |
|---|---|---|---|---|---|---|
| M-007 | Inline Sample Filtration SPE Column regenerated during analytical extraction | Analyst with ICC-CE | * TrioVS | * Automated filtration of sample on cleanup column prior to separation on analytical column | * No "Look Ahead" * Can not prep samples ahead of analytical run | No |
On-Line SPE Application Note from ABI for Pesticides in Drinking Water[1]
Contents |
Overview
This configuration allows the automated on-line Solid Phase Extraction (SPE). This is run directly from within Analyst Software[2] from Applied Biosystems Inc using a Standard LEAP Cycle (requires ICC-CE software) [3].
There are 2 pumps needed, one for the gradient run and another (higher flow rate and isocratic) for regeneration [4]. This configuration requires a TrioVS Valve [5]. All of the valves must be controlled by the Standard LEAP cycle.
LEAP can not control the MS Selector valve as part of the cycle.
Useful links
www.appliedbiosystems.com Application Note [6]
For other cost/time saving measures consider:
- LEAP offers multiple choices of Valve Self Wash Stations to aid in cleaning the valve [7]
- Summary of LC Multi Valve Applications [8]
- LEAP Shell Software and application for custom injections and scheduling [9]
Contact LEAP
For detailed information on In-line Sample Concentration or Filtration please contact LEAP Technologies
