EPA Method 8272
From LEAP
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Solid-Phase Microextraction: The SPME extraction of the water samples is performed using a commercially available polydimethylsiloxane (PDMS)-coated fused silica fiber while the water sample is mixed by the precession of the autosampler mixing chamber. | Solid-Phase Microextraction: The SPME extraction of the water samples is performed using a commercially available polydimethylsiloxane (PDMS)-coated fused silica fiber while the water sample is mixed by the precession of the autosampler mixing chamber. | ||
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| + | The EPA narcosis model for benthic organisms in sediments contaminated with polycyclic aromatic hydrocarbons (PAHs) is based on the concentrations of dissolved PAHs in the interstitial water or pore water in sediment. Method 8272 covers the separation of pore water from PAH-impacted sediment samples, the removal of colloids, and the subsequent measurement of dissolved concentrations of the 10-parent PAHs and two alkylated daughter PAHs in the pore water samples. This method directly determines the concentrations of dissolved PAHs in environmental sediment pore water, groundwater, and other water samples using solid-phase microextraction (SPME) for static sample collection followed by desorption into a gas chromatograph (GC) equipped with a mass spectrometric (MS) detector operated in the selected ion monitoring (SIM) mode for analyte identification and quantitation. | ||
=== Useful links === | === Useful links === | ||
Revision as of 12:26, 4 June 2010
| SEDIMENT PORE WATER BY SOLID-PHASE MICROEXTRACTION AND GAS CHROMATOGRAPHY/MASS SPECTROMETRY |
| Application Type | |
| SPME | |
| Application ID | |
| SPME on PAL | |
| Description | |
| EPA Method 8272 |
General Description
U.S. Environmental Protection Agency (USEPA) has method 8272 which is PARENT AND ALKYL POLYCYCLIC AROMATICS IN SEDIMENT PORE WATER BY SOLID-PHASE MICROEXTRACTION AND GAS CHROMATOGRAPHY/MASS SPECTROMETRY IN SELECTED ION MONITORING MODE. This method can be used to determine nanogram to milligram per liter PAH concentrations in pore water. The PAHs are determined using SPME followed by gas chromatography/mass spectrometry (GC/MS) analysis in selected ion monitoring (SIM) mode. Solid-Phase Microextraction: The SPME extraction of the water samples is performed using a commercially available polydimethylsiloxane (PDMS)-coated fused silica fiber while the water sample is mixed by the precession of the autosampler mixing chamber.
The EPA narcosis model for benthic organisms in sediments contaminated with polycyclic aromatic hydrocarbons (PAHs) is based on the concentrations of dissolved PAHs in the interstitial water or pore water in sediment. Method 8272 covers the separation of pore water from PAH-impacted sediment samples, the removal of colloids, and the subsequent measurement of dissolved concentrations of the 10-parent PAHs and two alkylated daughter PAHs in the pore water samples. This method directly determines the concentrations of dissolved PAHs in environmental sediment pore water, groundwater, and other water samples using solid-phase microextraction (SPME) for static sample collection followed by desorption into a gas chromatograph (GC) equipped with a mass spectrometric (MS) detector operated in the selected ion monitoring (SIM) mode for analyte identification and quantitation.
Useful links
The official method at EPA .gov
LEAP provides automated workstation instrumentation solutions based on the LEAP CTC PAL X, Y, Z syringe only autosampler robot from LEAP Technologies. This extremely flexible, precise, and adaptable liquid handling robotic platform is available in a variety of lengths and options depending on the requirements of your sample preparation and injections for your UHPLC, LC or GC chromatography.LEAP offers full support and service for the PAL platform in addition to being able to write custom macros, cycles, and scheduling to your applications. Please contact LEAP Technologies on how we can help you get maximized throughput with flexible pipetting automation solutions.
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