EN 14110 Methanol content by HS

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   Image:hs1.png  | Cycle Composer method parameters
   Image:hs1.png  | Cycle Composer method parameters
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  Image:6584SamplePrepISMSTFA.png | Cycle Composer Sample Prep
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  Image:CCSTD prep sample list.png  | Cycle Composer Prep Standards
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  Image:6584StandardsPrep.png | ChemStation Sequence Table
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  Image:SequencetableA.png | ChemStation Sequence Table
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  Image:1_ul_inj.png | ChemStation PAL Method for Injection
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  Image:GCInjfor6584.png | ChemStation and Cycle for injection
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== Video ==
 
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*[[:Image:DISPTool.ppt | Dispense Tool movement]]
 
== Useful links ==
== Useful links ==
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UCONN.com  A good general reference site on Biodiesel without buying the ASTM Methods [http://biodiesel.engr.uconn.edu/home/Stuart.pdf]
UCONN.com  A good general reference site on Biodiesel without buying the ASTM Methods [http://biodiesel.engr.uconn.edu/home/Stuart.pdf]
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www.biodiesel.org  A good general reference site on Biodiesel  [www.biodiesel.org]
Biodiesel Plant Listing [http://www.biodieselmagazine.com/plant-list.jsp]
Biodiesel Plant Listing [http://www.biodieselmagazine.com/plant-list.jsp]
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*[[:Image:EN14110.pdf‎ | EN 14110 - not for redistribution]]
*[[:Image:EN14110.pdf‎ | EN 14110 - not for redistribution]]
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== Other Reference material ==
 
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*[[:Image:LEAP_ASTM_D_6584_Quick_User_Guide_Rev_5.pdf‎  | ASTM D6584 - Quick User Guide]]
 

Revision as of 14:46, 9 February 2009

Biofuels
Application Type
  Sample Inject
Application ID
  Biodiesel EN14110
Description
  Determination of Methanol content by Headspace

Contents

Overview

EN14110 describes the required method for methanol determination in biodiesel.

Significant Markets

  • Biodiesel Manufactures
  • Biodiesel Blenders
  • Biodiesel Distributors
  • Biofuels CROs
  • Fleet Managers

EN Method 14110

9. Calibration and Standardization

9.2 Standard Solutions – Prepare the five standard solutions in Table 3 by transferring the specified volumes by means of Microliter syringes to 10mL septa vials. Add to each of the five standard solutions 100uL of MSTFA. Close the vial and shake. Allow the vial to stand for 15 to 20 minutes at room temperature. Add approximately 8 mL n-Heptane to vial and shake.

Photos

Representative System shown with Agilent 7890 and Combi PAL
Representative System shown with Agilent 7890 and Combi PAL



Software Control

Currently the COMBI PAL and runs on via the hand held due to the desire for look ahead funcationality.

Can also be run uncer Cycle Coposer or Agilent CTC cotrol software without look ahead fuctionality.


Screenshots


Useful links

Biodieselanalytical.com A good general reference site on Biodiesel automation theory and practice [1]

A good general reference site by Agilent [2]

UCONN.com A good general reference site on Biodiesel without buying the ASTM Methods [3]

www.biodiesel.org A good general reference site on Biodiesel [www.biodiesel.org]

Biodiesel Plant Listing [4]

Biodiesel Conference 2009 [5]

Publications

Personal tools