ASTM D 5453 Sulfur Content

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(New page: {{LSApp |name = Biofuels |image = 9000Series.png |type = Sample Prep and Inject |id = Biodiesel ASTM D 5453 |description = Sulfur }} === Overview ==...)
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=== Overview ===
=== Overview ===
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Gas chromatography can also serve as a tool for process troubleshooting during biodiesel production to ensure trouble-free operation of the fuel in diesel engines. Monitoring the level of free glycerin and any unrelated mono-, di-, and triglycerides will indicate the efficiency and progress of the chemical reaction during the process of making biodiesel.
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ASTM D 5453 is a proven method for the determination of sulfur in liquid hydrocarbons.
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ASTM Method D6584 provides for the quantitative determination of free and total glycerin in B-100 methyl esters by gas chromatography. The range of detection for free glycerin is 0.005 to 0.05 mass%, and total glycerin from 0.05 to 0.5 mass %. This method is not applicable to vegetable oil methyl esters obtained from lauric oils, such as coconut oil and palmkernel oil.
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Test Method ASTM D 5453
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* Limits: 0.05 % mass maximum
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* S oxidized to SO2 at high temperatures
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* UV phluorescence of emited gases
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* S limits dictated by environmental considerations
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* Limits vary according to State regulations
=== Significant Markets  ===
=== Significant Markets  ===
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* Fleet Managers
* Fleet Managers
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Also compatible with ASTM D 6667 and EN ISO 20846
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[[image:Download Icon.png|40px]] [http://www.antekhou.com/products%5C9000LLS%5CPDF%5CBrochure%5CEN%5C9000LLS%20rev1.pdf Antek - Complete Sulfur Analyzer ]
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Antek - Complete Sulfur Analyzer  [http://www.antekhou.com/products%5C9000LLS%5CPDF%5CBrochure%5CEN%5C9000LLS%20rev1.pdf]
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[[image:Download Icon.png|40px]] [http://www.paclp.com/products%5C9000NS%5CPDF%5CAppl_Note%5CEN%5C922%20-%20S%20and%20N%20in%20Palm%20oil.pdf Antek - Application Note]
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===Useful links ===
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[[Image:Www icon.png|40px]] [http://www.4cleanfuels.com/biofuels/BioDQuality8-07/FQ_workshop-PiedmontBioFuels.pdf An overview of all tests that must be run by Piedmont Biofuels]
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== Useful links ==
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[[Image:Www icon.png|40px]] [http://www.chem.agilent.com/cag/prod/GC/Biodiesel_QR.pdf A good general reference site by Agilent]
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[[Image:Www icon.png|40px]] [http://biodiesel.engr.uconn.edu/home/Stuart.pdf UCONN.com  A good general reference site on Biodiesel ASTM Methods]
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Biodieselanalytical.com   A good general reference site on Biodiesel automation theory and practice [http://biodieselanalytical.com/instsum.aspx]
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[[Image:Www icon.png|40px]] [http://www.biodiesel.orgwww.biodiesel.org   A good general reference site on Biodiesel ]
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An overview of all tests that must be run [http://www.4cleanfuels.com/biofuels/BioDQuality8-07/FQ_workshop-PiedmontBioFuels.pdf]
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[[Image:Www icon.png|40px]] [http://www.biodieselmagazine.com/plant-list.jsp Biodiesel Plant Listing ]
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A good general reference site by Agilent [http://www.chem.agilent.com/cag/prod/GC/Biodiesel_QR.pdf]
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[[Image:Www icon.png|40px]] [http://www.biodieselconference.org/2009/default.asp Biodiesel Conference 2009 ]
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UCONN.com  A good general reference site on Biodiesel ASTM Methods [http://biodiesel.engr.uconn.edu/home/Stuart.pdf]
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=== Videos of PAL ===
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<br>
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[[Image:Movie Icon.png|40px]]
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[http://www.youtube.com/user/LEAPTechnologies#g/u LEAP's PAL Application Videos on YouTube]
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<br>
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www.biodiesel.org  A good general reference site on Biodiesel  [http://www.biodiesel.org]
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{{logo}}
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This workstation application is based on the CTC PAL X, Y, Z syringe only autosampler robot from LEAP Technologies. This extremely flexible, precise, and adaptable robotic platform is available in a variety of lengths and options depending on the requirements of your sample preparation and injections for your LC or GC requirements. Please contact LEAP Technologies on how we can help you get maximized throughput with flexible automation.
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Biodiesel Plant Listing [http://www.biodieselmagazine.com/plant-list.jsp]
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=== Contact LEAP ===
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{{contact|topic=the PAL and the application}}
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Biodiesel Conference 2009 [http://www.biodieselconference.org/2009/default.asp]
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[[Category: Biofuel]]
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[[Category:Application_Solutions]]

Current revision

Biofuels
Application Type
  Sample Prep and Inject
Application ID
  Biodiesel ASTM D 5453
Description
  Sulfur
 ↳ leaptec.com  ↳ leapwiki.com

Contents

Overview

ASTM D 5453 is a proven method for the determination of sulfur in liquid hydrocarbons.

Test Method ASTM D 5453

  • Limits: 0.05 % mass maximum
  • S oxidized to SO2 at high temperatures
  • UV phluorescence of emited gases
  • S limits dictated by environmental considerations
  • Limits vary according to State regulations

Significant Markets

  • Biodiesel Manufactures
  • Biodiesel Blenders
  • Biodiesel Distributors
  • Biofuels CROs
  • Fleet Managers


Also compatible with ASTM D 6667 and EN ISO 20846

Antek - Complete Sulfur Analyzer


Antek - Application Note

Useful links

An overview of all tests that must be run by Piedmont Biofuels

A good general reference site by Agilent

UCONN.com A good general reference site on Biodiesel ASTM Methods

A good general reference site on Biodiesel

Biodiesel Plant Listing

Biodiesel Conference 2009

Videos of PAL


LEAP's PAL Application Videos on YouTube


 ↳ leaptec.com  ↳ leapwiki.com

This workstation application is based on the CTC PAL X, Y, Z syringe only autosampler robot from LEAP Technologies. This extremely flexible, precise, and adaptable robotic platform is available in a variety of lengths and options depending on the requirements of your sample preparation and injections for your LC or GC requirements. Please contact LEAP Technologies on how we can help you get maximized throughput with flexible automation.

Contact LEAP

Contact LEAP

For additional information about the PAL and the application, please contact LEAP Technologies.

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