EN 14110 Methanol content by HS
From LEAP
Line 8: | Line 8: | ||
=== Overview === | === Overview === | ||
- | + | EN14110 describes the required method for methanol determination in biodiesel. | |
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
=== Significant Markets === | === Significant Markets === | ||
Line 27: | Line 21: | ||
* Fleet Managers | * Fleet Managers | ||
- | ''' | + | '''EN Method 14110''' |
'''9. Calibration and Standardization''' | '''9. Calibration and Standardization''' | ||
Line 33: | Line 27: | ||
'''9.2 Standard Solutions''' – Prepare the five standard solutions in ''Table 3'' by transferring the specified volumes by means of Microliter syringes to 10mL septa vials. Add to each of the five standard solutions 100uL of MSTFA. Close the vial and shake. Allow the vial to stand for 15 to 20 minutes at room temperature. Add approximately 8 mL n-Heptane to vial and shake. | '''9.2 Standard Solutions''' – Prepare the five standard solutions in ''Table 3'' by transferring the specified volumes by means of Microliter syringes to 10mL septa vials. Add to each of the five standard solutions 100uL of MSTFA. Close the vial and shake. Allow the vial to stand for 15 to 20 minutes at room temperature. Add approximately 8 mL n-Heptane to vial and shake. | ||
- | + | === Photos === | |
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | [[Image:HP6890.jpg|200px|thumb|left|Representative System shown with Agilent 7890 and Combi PAL]] | |
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | + | ||
- | [[Image: | + | |
- | |||
- | |||
- | + | === Software Control === | |
- | + | Currently the COMBI PAL and runs on via the hand held due to the desire for look ahead funcationality. | |
- | + | ||
- | + | Can also be run uncer Cycle Coposer or Agilent CTC cotrol software without look ahead fuctionality. | |
- | + | ||
- | + | ||
- | + | ||
- | |||
Line 88: | Line 44: | ||
<gallery> | <gallery> | ||
- | Image: | + | Image:hs1.png | Cycle Composer method parameters |
Image:6584SamplePrepISMSTFA.png | Cycle Composer Sample Prep | Image:6584SamplePrepISMSTFA.png | Cycle Composer Sample Prep | ||
Image:CCSTD prep sample list.png | Cycle Composer Prep Standards | Image:CCSTD prep sample list.png | Cycle Composer Prep Standards |
Revision as of 14:44, 9 February 2009
Biofuels | |
Application Type | |
Sample Inject | |
Application ID | |
Biodiesel EN14110 | |
Description | |
Determination of Methanol content by Headspace |
Contents |
Overview
EN14110 describes the required method for methanol determination in biodiesel.
Significant Markets
- Biodiesel Manufactures
- Biodiesel Blenders
- Biodiesel Distributors
- Biofuels CROs
- Fleet Managers
EN Method 14110
9. Calibration and Standardization
9.2 Standard Solutions – Prepare the five standard solutions in Table 3 by transferring the specified volumes by means of Microliter syringes to 10mL septa vials. Add to each of the five standard solutions 100uL of MSTFA. Close the vial and shake. Allow the vial to stand for 15 to 20 minutes at room temperature. Add approximately 8 mL n-Heptane to vial and shake.
Photos
Software Control
Currently the COMBI PAL and runs on via the hand held due to the desire for look ahead funcationality.
Can also be run uncer Cycle Coposer or Agilent CTC cotrol software without look ahead fuctionality.
Screenshots
Video
Useful links
Biodieselanalytical.com A good general reference site on Biodiesel automation theory and practice [1]
A good general reference site by Agilent [2]
UCONN.com A good general reference site on Biodiesel without buying the ASTM Methods [3]
Biodiesel Plant Listing [4]
Biodiesel Conference 2009 [5]